
Differential Scanning Calorimeter (DSC) from TA Inst. Co., measures the difference in heat absorbed or released by sample, as compared to an inert refference (empty pan), as both are heated, cooled or held at constant temperature (isothermal). Exothermic transitions result in the release of heat: crystallization, curing, decomposition, etc. Endothermic transitions absorb heat: melting, glass transition, evaporation, etc. DSC Q-2000 using the Tzero technique provides significant improvements in baseline flatness, transition, resolution and sensitivity.
Equipment
Instrument: TA Instruments Q2000 DSC with 50 position autosampler. Sensitivity < 0.2 µW, and baseline drift < 10 µW.
Temperature: from – 170 °C to 400 °C (please check stability of the polymer using TGA). Liq Nitrogen cooling system.
Calibration: Indium. Sapphire was used for heat capacity constant.
Lab:
Location:
MRL room 1052
Manufacturer's Info:
TA Instruments
109 Lukens Dr.
New Castle, DE 19720
Telephone: 302-427-4000
Fax: 302-427-4041
Email: answerman [at] tainst [dot] com
Internet - http://www.tainstruments.com
Application Hotline: 302-427-4070
Instrument Information and/or Manual:
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Contact:
Please contact Rachel Behrens (rachel [at] mrl [dot] ucsb [dot] edu) to schedule training. Before training starts please read the online MANUAL and view the online presentation.